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ASTM International, 06/15/2013
Publisher: ASTM
File Format: PDF
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Published:15/06/2013
Pages:10
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1.1 This practice covers the procedure for use of microwave radiation for sample decomposition prior to elemental determination by atomic spectroscopy.
1.1.1 Although this practice is based on the use of inductively coupled plasma atomic emission spectrometry (ICP-AES) and atomic absorption spectrometry (AAS) as the primary measurement techniques, other atomic spectrometric techniques may be used if lower detection limits are required and the analytical performance criteria are achieved.
1.2 This practice is applicable to both petroleum products and lubricants such as greases, additives, lubricating oils, gasolines, and diesels.
1.3 Although not a part of Committee D02's jurisdiction, this practice is also applicable to other fossil fuel products such as coal, fly ash, coal ash, coke, and oil shale.
1.3.1 Some examples of actual use of microwave heating for elemental analysis of fossil fuel products and other materials are given in Table 1.
Material
Element(s) Determined
Measurement Technique
ReferenceA
Biological Materials
Multiple
AAS and NAA
Abu Samra et al (1)
Barrett et al (2)
West et al (3)
Geological Materials
Matthes et al (4)
Oil Shales
ICP-AES
Nadkarni (5)
Coal and Fly Ash
Plant and Grain Standards
ICP-MS
Feng et al (6)
Greases
Fox (7); Nadkarni (8)
Petroleum Products
Hwang et al (9)
Crude Oil
Xie et al (10)
Residual Fuel Oil
Wondimu et al (11)
Oils
Lanthanides and Platinum Group Metals
Woodland et al (12)
AAS; ICP-AES
Kingston and Jassie (13)
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